Recent Advances in Solid-State Nuclear Magnetic Resonance Techniques for Materials Research

Annual Review of Materials Research

Vol. 50:493-520 (Volume publication date July 2020)
First published as a Review in Advance on May 15, 2020
https://doi.org/10.1146/annurev-matsci-091019-011049

Abstract

Establishing structure–property correlations is of paramount importance to materials research. The ability to selectively detect observable magnetization from transitions between quantized spin states of nuclei makes nuclear magnetic resonance (NMR) spectroscopy a powerful probe to characterize solids at the atomic level. In this article, we review recent advances in NMR techniques in six areas: spectral resolution, sensitivity, atomic correlations, ion dynamics, materials imaging, and hardware innovation. In particular, we focus on the applications of these techniques to materials research. Specific examples are given following the general introduction of each topic and technique to illustrate how they are applied. In conclusion, we suggest future directions for advanced solid-state NMR spectroscopy and imaging in interdisciplinary research.

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